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Beilstein J. Org. Chem. 2014, 10, 2981–2988, doi:10.3762/bjoc.10.316
Graphical Abstract
Figure 1: Examples of biologically active 1,2-disubstituted tetrahydroisoquinolines.
Scheme 1: Oxidative C–H functionalisation and examples of previously reported nucleophilic trappings.
Figure 2: Products from allylzinc reagent addition to 5a and 5b.
Figure 3: Proposed mechanism for formation of side-product 8a. Analogous reactivity in the formation of cycli...
Figure 4: Mechanism for dimerisation of the allylzinc halide and β-hydride addition to 5a [36].
Scheme 2: A concise synthesis of methopholine (3).